The three control samples, the approximate ages of which were made known to the laboratories, are listed below. T/32) from a tomb excavated at Qasr Ibrîm in Nubia by Professor J. This linen was dated in the British Museum Research Laboratory using liquid scintillation counting, giving a radiocarbon age of 2,010 ± 80 yr BP (BM-2558).Two were in the form of whole pieces of cloth (samples 2 and 3) and one was in the form of threads (sample 4). This corresponds to a calendar age, rounded to the nearest 5 years, of 110 cal BC - AD 75 cal at the 68 per cent confidence level (where cal denotes calibrated radiocarbon dates). Threads removed from the cope of St Louis d'Anjou which is held in a chapel in the Basilica of Saint-Maximin, Var, France.Testore of Department of Materials Science, Turin Polytechnic and G. If the samples had been unravelled or shredded rather than being given to the laboratories as whole pieces of cloth, then it would have been much more difficult, but not impossible, to distinguish the shroud sample from the controls.Vial of Musée des Tissues and Centre International d'Étude des Textiles Anciens in Lyon), Dr M. Tite of the British Museum, representatives of the three radiocarbon-dating laboratories (Professor P. (With unravelled or shredded samples, pretreatment cleaning would have been more difficult and wasteful.) Because the shroud had been exposed to a wide range of potential sources of contamination and because of the uniqueness of the samples available, it was decided to abandon blind-test procedures in the interests of effective sample pretreatment.Photography of the shroud by Secondo Pia in 1898 indicated that the image resembled a photographic 'negative' and represents the first modern study.Subsequently the shroud was made available for scientific examination, first in 19 by a committee appointed by Cardinal Michele Pellegrino .The Arizona group split each sample into four subsamples.One pair of subsamples from each textile was treated with dilute HCL, dilute Na OH and again in acid, with rinsing in between (method a).
Also, at two laboratories (Oxford and Zurich), after combustion to gas, the samples were recoded so that the staff making the measurements did not know the identity of the samples. On the basis of the Islamic embroidered pattern and Christian ink inscription, this linen could be dated to the eleventh to twelfth centuries AD. Linen from the collection of the Department of Egyptian Antiquities at the British Museum, associated with an early second century AD mummy of Cleopatra from Thebes (EA6707).Among those present when the sample as cut from the shroud were Cardinal Anastasio Ballestrero (Archbishop of Turin), Professor L. The laboratories were not told which container held the shroud sample.Gonella (Department of Physics, Turin Polytechnic and the Archbishop's scientific adviser), two textile experts (Professor F. Because the distinctive three-to-one herringbone twill weave of the shroud could not be matched in the controls, however, it was possible for a laboratory to identify the shroud sample.Zurich precleaned the sample in an ultrasonic bath.After these initial cleaning procedures, each laboratory split the samples for further treatment.
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All laboratories examined the textile samples microscopically to identify and remove any foreign material.